ASTM E478 PDF
Published September Origi- nally approved in Last previous edition approved in as 3. E – 89a (). Annual Book of ASTM Standards. Buy ASTM E TEST METHODS FOR CHEMICAL ANALYSIS OF COPPER ALLOYS from SAI Global. These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for.
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However, in a cooperative program conducted by six laboratories, the results reported in Asm 9 were obtained. Refer to Section 6 of Practices E Aluminum is chelated with an excess of a standard solution of disodium ethylenedinitrilo tetraacetate EDTA and then determined by back-titration with standard zinc solution. Cover the beaker and heat until dissolution is complete.
ASTM E – 08() Standard Test Methods for Chemical Analysis of Copper Alloys
Proceed to Checkout Continue Shopping. Using a pH meter, check the pH of the solution which should be between 5. Allow to stand for 30 min and proceed as directed in A cathode of these dimensions will have a surface area of cm 2 exclusive of the stem.
If dissolution is difficult, add 0. When dissolution is complete, heat the solution to boiling and continue to boil until oxides of nitrogen are removed.
For low levels of lead, expanded scale readout is advisable. Subscription pricing is determined by: Gauze cathodes are recommended, and shall be made preferably from mesh gauze woven from wire approximately 0. The extraction procedure also affords a separation of the zinc from cadmium. Calculate the percentage of iron as follows: Proceed as directed in Do not use a solution that has stood more than 1 day. Although samples with the nickel concentration near the upper limit of the scope were not available for testing, the precision data obtained for the other specimens should apply.
No other units of measurement are included in this standard.
Store in a tightly closed polyethylene dropping bottle. After the blue color due to copper has disappeared, wash the cover glasses, electrodes, and the sides of the beaker, and continue the electrolysis until deposition of the copper is complete, as indicated by failure to plate on a new surface when the level of the solution is raised. Land Use and Development. Determine the appropriate concentration range as directed in Dilute to volume and mix. The surface of the platinum electrodes should be smooth, clean and bright to promote uniform deposition and good adherence.
Standard Test Methods for Chemical Analysis of Copper Alloys
Standards Subscriptions from ANSI provides a money-saving, multi-user solution for accessing standards. Prepare fresh prior to use. If no precipitate forms, proceed as directed in Users are encouraged to use this or similar reference materials to verify that the method is performing accurately in their laboratories. Dilute the aliquot to mL and proceed as directed in Heat to copious white fumes to volatilize the tin.
Prepare fresh as needed.
ASTM E478 – 08(2017)
The copper oxalyldihydrazide complex is formed with the copper remaining in the electrolyte. The over-all height of the cathode should be approximately mm. Originally na lly ap appro prove vedd in 19 When dissolution is e4788, boil for 1 min to destroy excess peroxide, and cool. Retain the organic layer.
Discard the organic layer.